Cyclopropylcarbinol

Name: Cyclopropylcarbinol
Availability: cyclopropylcarbinol-296753.html

Category:Intermediates
Product Name:Cyclopropylcarbinol
CAS No.:2516-33-8
Standard:USP
Price(USD):Negotiable
Company:Chongqing Xingcan Pharmaceutical Technology Co., Ltd.

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Basic Info

Grade: pharmaceutical grade

Factory Location: china

Main Sales Markets: North America,Central/South America,Western Europe,Eastern Europe,Australasia,Eastern Europe,Australasia,Asia,Middle East,Africa
Packaging Information: 1kg/bag
Sample Provided: no

Payment Terms: Bank transfer

In a glove box filled with nitrogen, add Ru catalyst (1 mol%), amide (1.0 mmol), potassium tert-butoxide (1.2 mol%), and tetrahydrofuran (2 mL) to a 100 mL pressure-resistant tube, replace the air in the pressure-resistant tube with hydrogen (30 psi three times), and add Chemicalbook pressure with H2 (14atm). After placing the reaction tube in a protective cover, stir at a constant temperature for 36h in a reaction oil bath at 110 °C. After the reaction, the reaction system is cooled to room temperature, excess H2 is carefully discharged, and the solvent is removed under reduced pressure. Purification of the product by Kugelrohr distillation or column chromatography yields the target product molecule, hydroxymethylcyclopropane.

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